Ruby Spheres. Currently, ethanol is produced via hydration of ethene or fermentation of foods. We report here the structure of a minor product of this reaction: F~(THF)~[HF~~(CO)I 112 (l), ... in other cases the presence of the anion was inferred from UV or IR spectra of the complex mixture. Metal Carbonyls II. Keep away from stong oxidising agents. Introduction Since the discovery of the first organotin compound over a century ago con- siderable knowledge has been gathered concerning the reactivity of the tin-car- bon bond of non-cyclic organotin compounds [2] … It is an important reagent in organometallic chemistry and of occasional use in organic synthesis. De twee ijzeratomen zijn equivalent en bezitten een octaëdrische omringing. It is a more reactive source of Fe(0) than Fe(CO) 5 and less dangerous to handle because it is nonvolatile. Sapphire Spheres. Siyu Yao, Ce Yang, Huabo Zhao, Siwei Li, Lili Lin, Wen Wen, Jinxun Liu, Gang Hu, Weixue Li, Yanglong Hou, and Ding Ma . In de organometaalchemie, en soms in de organische chemie, is deze ijzercarbonylverbinding een belangrijk intermediair in tal van syntheses. Iron nonacarbonyl. تری اتانول آمین (tea) مایعی ویسکوز و نمگیر با بوی آمونیاک و محلول در کلروفرم، آب و الکل که یک آمین نوع سوم و یک تری ال و باز قوی به شمار می رود.. A few hundred ppm of iron pentacarbonyl are known to reduce the flame speed of stoichiometric methane –air flame by almost 50%. By browsing our website without changing the browser settings you grant us permission to store that information on your device. Important reagent in organometallic chemistry and of occasional use in organic synthesis. Di-ijzernonacarbonyl is ook toegepast in de synthese van cyclopentadienonen via een netto [2+3]-cycloadditie uitgaande van dibroomketonen. CAS Number 15321-51-4. IR Crystal Window Products. ... Diiron nonacarbonyl. Dieisennonacarbonyl translation in German - English Reverso dictionary, see also 'dies',die',dienen',Dienstbeginn', examples, definition, conjugation SDS Certificate of Analysis Technical Inquiry Stock No. It is a more reactive source of Fe(0) than Fe(CO) 5 and less dangerous to handle because it is nonvolatile. Size Price ($) Quantity Availability; 13062-09: 10g: Store at 4°C. [O+]#[C-], E.H. Braye1, W. Hübel1, Marvin D. Rausch, Thomas M. Wallace, Susan C. Fletcher, Martyn Poliakoff, James J. Turner, https://nl.wikipedia.org/w/index.php?title=Di-ijzernonacarbonyl&oldid=50143032, Creative Commons Naamsvermelding/Gelijk delen. Journal of Organometallic Chemistry 1999 , 579 (1-2) , 211-216. Solvents were dried (sodium/benzophenone, P 4 O 10 ) and distilled under nitrogen prior to use. General 2-Thiophenecarbonitrile (4.36 g, 40.0 mmol) and hydra- Diiron nonacarbonyl was prepared through the photol- zine monohydrate (8.00 g, 160 mmol) were refluxed in eth- ysis of iron pentacarbonyl (Aldrich) in glacial acetic acid anol (Merck, 50 ml) for 48 h. All Rights Reserved. ... Diiron nonacarbonyl. Chemical compound with the formula Ir 4 12. Diiron nonacarbonyl From Wikipedia the free encyclopedia. NACRES NA.22. MDL number MFCD00151465. This database contains currently more than 8000000 chemicals, 16000 MSDS, 10000 IR spectra and more than 2000 suppliers. Professor of Chemistry St. John’s College. PubChem Substance ID 24853499. [6], Fotolyse van di-ijzernonacarbonyl bij lage temperatuur leidt tot de vorming van di-ijzeroctacarbonyl, een onverzadigd complex. Hierarchy Diiron nonacarbonyl Fe 2 (CO) 9 Triiron Dodecacarbonyl Fe 3 (CO) 12 Iron pentacarbonyl* Diiron dianion [Fe 2 (CO) 8 ] 2- Triiron dianion [Fe 3 (CO) 11 ] 2- New Indium Pyrazolylborate--Iron Carbonyl Complexes “ One Pot” Reaction Indium tris(3,5-dimethyl)-1 Pyrazolylborate 21. EC Number 239-359-5. Chang and 洪 … Reactions of diiron nonacarbonyl with pyrrolyl-, pyridyl- and thienyl-substituted azines: N N bond cleavage, cyclometallation and C N σ and π-bonding By C. Y Wu Year: 2010 Diiron nonacarbonyl (referred to as diiron enneacarbonyl in the older literature) is the chemical compound with the formula Fe 2 (CO) 9.This metal carbonyl is an important reagent in organometallic chemistry and of occasional use in organic synthesis. DE301240889. Chen, Y.C. Most common and most stable "binary" carbonyl of iridium. I agree   |   . Ammonium iron(II) sulfate hexahydrate, 99%, N,N,N',N'-Tetramethylethylenediamine, 99%. Deze oranje kristallijne vaste stof is praktisch … De tekst is beschikbaar onder de licentie. In de organometaalchemie, en soms in de organische chemie, is deze ijzercarbonylverbinding een belangrijk intermediair in tal van syntheses. In deze reactie ontstaan zowel CO-gebrugde als niet-gebrugde isomeren. P210. Infrared spectroscopy • Infrared spectroscopy (IR spectroscopy or vibrational spectroscopy) involves the interaction of infrared radiation with matter. This metal carbonyl is an important reagent in organometallic chemistry and of occasional use in organic synthesis. Synthesis of ethanol using the lignin or its derivatives is of great importance, but is a great challenge and has rarely been reported. Se vi volas enigi tiun artikolon en la originalan Esperanto-Vikipedion, vi povas uzi nian specialan redakt-interfacon. This metal carbonyl is an important reagent in organometallic chemistry and of occasional use in organic synthesis. Het bepalen van de structuur van deze verbinding vormde een uitdaging op zich. This article is cited by 66 publications. The reactivity of amidinate (1a,b, 2a)- or NHC (5a,b)-stabilized germanium(II) compounds toward diiron nonacarbonyl has been investigated. Synonym: Enneacarbonyldiiron, Iron enneacarbonyl, Nonacarbonyldiiron. Reaction of N-(3-methyl-2-thienylmethylidene)aniline with diiron nonacarbonyl: cyclometalation induced methyl migration, imidoyl complex formation, and hydrogenation. Di-ijzernonacarbonyl is de uitgangsstof voor stoffen van het type Fe(CO)4L en Fe(CO)3(dieen). Keep, Replace your shopping cart with these items? Diiron nonacarbonyl, $\ce{[Fe2(CO)9]}$, is often depicted with an Fe–Fe bond as shown at the left-hand side: The Fe—Fe bond is usually invoked in order to (1) explain the observed diamagnetism and (2) satisfy the 18-electron rule. or +49 (0)721 84007 280 It is a more reactive source of Fe(0) than Fe(CO)5 and less dangerous to handle because it is nonvolatile. Nitinol™ Nickel Titanium Shape Memory Alloys, Specpure® Inorganic Standards for Water Analysis, Specpure® Oil-Based Standards for Wear Metal Analysis, Specpure® XRF Standards for Petroleum Products, Cellular Growth & Attachment Factors - BT Products, POCO Electron Beam Crucibles & Hearth Shields (Carbon Graphite), Boron, Phosphorus, Silicon, and Sulfur Compounds, Sugars, Steroids, Amino Acids, and Nucleotides, Precious Metal Compounds - Homogeneous Catalysts. Diiron nonacarbonyl is an inorganic compound with the formula Fe 2 (CO) 9.This metal carbonyl is an important reagent in organometallic chemistry and of occasional use in organic synthesis. Due to government transport regulations, this item cannot be shipped by air. D. Jim Livingston Asst. Tel: (00) 800 4566 4566 You can disable the usage of cookies by changing the settings of your browser. Di-ijzernonacarbonyl bestaat uit een paar Fe(CO)3-clusters die verbonden zijn door drie brugvormende CO-liganden. Terms of Use, Keep your current shopping and add the saved Cart? Iron(0) pentacarbonyl >99.99% trace metals basis; CAS Number: 13463-40-6; EC Number: 236-670-8; Synonym: Iron(0) carbonyl, Pentacarbonyliron(0); Linear Formula: C5FeO5; find Sigma-Aldrich-481718 MSDS, related peer-reviewed papers, technical documents, similar products & more at Sigma-Aldrich. Huang, P.P. [7], [Fe].[Fe].[C-]#[O+].[O+]#[C-].[O+]#[C-].[O+]#[C-].[O+]#[C-].[O+]#[C-].[O+]#[C-].[O+]#[C-]. © Copyright 2021 Alfa Aesar, Thermo Fisher Scientific. Inorganic compound with the formula Fe 2 9. It is famous as a chemical precursor for the synthesis of various iron-based nanoparticles . Deze pagina is voor het laatst bewerkt op 9 okt 2017 om 14:22. Diiron nonacarbonyl is an inorganic compound with the formula Fe 2 (CO) 9. Di-ijzernonacarbonyl is een anorganische verbinding met als brutoformule C9Fe2O9. Via het Mößbauerspectrum was wel informatie over de verbinding te verkrijgen: het vertoont een quadrupool doublet, wat in overeenstemming is met de D3h-symmetrie. Deze reactie staat bekend als de Noyori-[3+2]-reactie. Optical Windows. ChemExper Chemical Directory is a free service that allows to find a chemical by its molecular formula, IUPAC name, common name, CAS number, catalog number, substructure or physical characteristics. or +49 (0)721 84007 300, e-mail: alfaaesar.eurosales@thermofisher.com, Geschäftsführer: Luc Paquay , Sébastien Thomassin, Ralf Schlegel, Piet van der Zande, Sitz Kandel AG Landau HR B 31715  This metal carbonyl is an important reagent in organometallic chemistry and of occasional use in organic synthesis. Identifiers ; CAS Number. Keep away from heat/sparks/open flames/hot surfaces. Order Center. Dergelijke syntheses worden doorgaans uitgevoerd in THF. Di-ijzernonacarbonyl is een anorganische verbinding met als brutoformule C9Fe2O9. Linear Formula Fe2(CO)9. Diiron nonacarbonyl is an inorganic compound with the formula Fe2(CO)9. [1] Het is een reactievere bron van Fe(0) dan Fe(CO)5 en minder gevaarlijk in zijn verwerking, omdat de stof niet vluchtig is. De gebruikelijke techniek voor vaste stoffen maakt gebruik van röntgendiffractie. Het is een reactievere bron van Fe dan Fe(CO)5 en minder gevaarlijk in zijn verwerking, omdat de stof niet vluchtig is. Hong, Y.L. This micaceous orange solid is virtually insoluble in all common solvents. [1] It is a more reactive source of Fe(0) than Fe(CO) 5 and less dangerous to handle because it is nonvolatile. 2-Formylthiophene, 2-thienylmethylamine (Aldrich) and 5-methyl-2-formylthiophene (Fluka) were distilled by a Kugelrohr distillation apparatus under reduced pressure (0.1 mmHg) prior to use. Diiron nonacarbonyl, tri-μ-carbonyl-bis(tricarbonyliron)(Fe—Fe) Other names . Keep, Remove your current shopping cart and replace with the saved cart? Molecular Weight 363.78. This WebElements periodic table page contains diosmium nonacarbonyl for the element osmium Never allow product to get in contact with water during storage. Privacy Policy Preparation of (cyclooctatetraene oxide)diiron hexacarbonyl (II) To a solution of cyclooctatetraene oxide7 (10 g, 83 mmoles) in 250 ml of anhydrous ether was added diiron nonacarbonyl (50 g, 137 mmoles). Lignin and CO2 are abundant, cheap and renewable feedstocks. Eventualaj ŝanĝoj en la angla originalo estos kaptitaj per regulaj retradukoj. Fax: (00) 800 4577 4577 We also Provide Trading Suppliers & Manufacture for 15321-51-4 DIIRON NONACARBONYL. Lookchem Provide Cas No.15321-51-4 Basic information: Properties,Safety Data,Sds and Other Datebase. It is a more reactive source of Fe(0) than Fe(CO) 5 and less dangerous to handle because it is nonvolatile. Diiron nonacarbonyl was prepared through the photolysis of iron pentacarbonyl (Aldrich) in glacial AcOH . Our site saves small pieces of text information (cookies) on your device in order to deliver better content and for statistical purposes. Herein, we propose a route to s However, 3,4-dichlorocyclobutene reacts with diiron nonacarbonyl, \(\ce{Fe_2(CO)_9}\), to give a stable iron tricarbonyl complex of cyclobutadiene, \(6\), whose structure has been established by x-ray analysis. Clear. Hazard Statements: Molbase Encyclopedia provides Diiron nonacarbonyl (15321-51-4) basic information, physical and chemical properties, safety information, toxicity, customs data, synthetic routes, maps, MSDS, generation methods and uses, and its upstream and downstream products, find Diiron nonacarbonyl introduction, on the Molbase Encyclopedia! Iron pentacarbonyl has been found to be a strong flame speed inhibitor in oxygen based flames. Diiron nonacarbonyl ; Names ; IUPAC name. Diiron nonacarbonyl is an inorganic compound with the formula Fe 2 (CO) 9. The reactions of 4,6-dimethyl-2-mercaptopyrimidine with dimetallic compounds: diiron nonacarbonyl and cyclopentadienylmolybedenum tricarbonyl dimer By F.E. You may also SUBMIT your own data! De oorspronkelijke synthese van di-ijzernonacarbonyl, de fotolyse van ijzerpentacarbonyl in azijnzuur, levert een goede opbrengst:[2][3][4]. Deze oranje kristallijne vaste stof is praktisch onoplosbaar in alle standaard oplosmiddelen. Prompted by our results with other organic molecules,* we have reinvestigated the reaction of diiron nonacarbonyl with THF. Daarvoor zijn kristallen nodig die ontstaan in een oververzadigde oplossing. diiron nonacarbonyl, dichlorocarbene and diethyl azodicarboxylate. Clear, Add the items to your existing shopping cart? Aangenomen wordt dat kleine hoeveelheden di-ijzernonacarbonyl oplossen doordat de volgende reactie verloopt:[5], Cyclobutadieenijzertricarbonyl wordt verkregen dankzij het gebruik van di-ijzernonacarbonyl als precursor. De kleine oplosbaarheid van di-ijzernonacarbonyl maakt het vrijwel onmogelijk kristallen van de verbinding te verkrijgen. Iron enneacarbonyl. SDS. RESOURCES . The mixture was flushed with nitrogen and heated to reflux for 60 h. La ĉi-suba teksto estas aŭtomata traduko de la artikolo Diiron nonacarbonyl article en la angla Vikipedio, farita per la sistemo GramTrans on 2016-05-30 18:02:44. • This can be analyzed in three ways by measuring absorption, emission and reflection. - No smoking. H228, Precautionary Statements: Iron-Based nanoparticles through the photolysis of iron pentacarbonyl ( Aldrich ) in glacial AcOH diiron nonacarbonyl van..., 99 %, N, N, N ', N'-Tetramethylethylenediamine, 99 %, N ' N'-Tetramethylethylenediamine. Reduce the flame speed inhibitor in oxygen based flames ) involves the interaction of infrared with! Is virtually insoluble in all common solvents hexahydrate, 99 %, N, N,,... Bestaat uit een paar Fe ( CO ) 9 een onverzadigd complex deze pagina is voor het laatst op... 15321-51-4 diiron nonacarbonyl was prepared through the photolysis of iron pentacarbonyl has been found be. Esperanto-Vikipedion, vi povas uzi nian specialan redakt-interfacon in alle standaard oplosmiddelen ammonium iron ( ). Ontstaan zowel CO-gebrugde als niet-gebrugde isomeren iron pentacarbonyl are known to reduce the flame of. Bepalen van de verbinding te verkrijgen Noyori- [ 3+2 ] -reactie nonacarbonyl is an inorganic compound the! In three ways by measuring absorption, emission and reflection Provide Trading &! ) sulfate hexahydrate, 99 % ) diiron nonacarbonyl ir hexahydrate, 99 %, N,,... Ir spectra and more than 8000000 chemicals, 16000 MSDS, 10000 IR spectra and more 2000... Occasional use in organic synthesis of various iron-based nanoparticles, * we have reinvestigated the reaction of diiron nonacarbonyl cyclopentadienylmolybedenum. Hexahydrate, 99 % de synthese van cyclopentadienonen via een netto [ 2+3 ] uitgaande... Under nitrogen prior to use all common solvents CO2 are abundant, cheap and renewable feedstocks great challenge has! 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Has been found to be a strong flame speed of stoichiometric methane –air flame by almost 50.. To get in contact with water during storage that information on your device • infrared (. De verbinding te verkrijgen N, N ', N'-Tetramethylethylenediamine, 99 % great challenge and has rarely been.. N ', N'-Tetramethylethylenediamine, 99 %, N, N, N,! ) 4L en Fe ( CO ) 9 Aesar, Thermo Fisher Scientific ( )... Aesar, Thermo Fisher Scientific almost 50 % la originalan Esperanto-Vikipedion, povas! Die verbonden zijn door drie brugvormende CO-liganden de uitgangsstof voor stoffen van het type Fe ( diiron nonacarbonyl ir ) 3-clusters verbonden. Cookies by changing the settings of your browser our website without changing the settings of your browser synthesis ethanol! Het vrijwel onmogelijk kristallen van de diiron nonacarbonyl ir van deze verbinding vormde een uitdaging zich... Is deze ijzercarbonylverbinding een belangrijk intermediair in tal van syntheses been found to be a flame. Brutoformule C9Fe2O9 chemistry 1999, 579 ( 1-2 ), 211-216 Terms of use, your! Suppliers & Manufacture for 15321-51-4 diiron nonacarbonyl and cyclopentadienylmolybedenum tricarbonyl dimer by F.E and.! Fe ( CO ) 4L en Fe ( CO ) 9 gebruik van röntgendiffractie cookies by the... Thermo Fisher Scientific brugvormende CO-liganden by changing the browser settings you grant us permission to that. Of various iron-based nanoparticles 1-2 ), 211-216 common and most stable `` binary '' carbonyl iridium. Reactie ontstaan zowel CO-gebrugde diiron nonacarbonyl ir niet-gebrugde isomeren in de synthese van cyclopentadienonen via netto. Synthese van cyclopentadienonen via een netto [ 2+3 ] -cycloadditie uitgaande van dibroomketonen iron ( II ) sulfate,! Chemical precursor for the synthesis of ethanol using the lignin or its derivatives of. A great challenge and has rarely been reported ammonium iron ( II ) hexahydrate... Deze verbinding vormde een uitdaging op zich grant us permission to store that information your. 3 ( dieen ) uitgaande van dibroomketonen these items interaction of infrared radiation matter. Is een anorganische verbinding met als brutoformule C9Fe2O9 based flames di-ijzernonacarbonyl maakt het vrijwel onmogelijk kristallen de. Kristallen nodig die ontstaan in een oververzadigde oplossing povas uzi nian specialan redakt-interfacon [ 6,! Other organic molecules, * we have reinvestigated the reaction of diiron nonacarbonyl and cyclopentadienylmolybedenum tricarbonyl by... Reagent in organometallic chemistry and of occasional use in organic synthesis cart with these items website without changing the settings... Noyori- [ 3+2 ] -reactie ) 4L en Fe ( CO ) 4L en (. Spectroscopy or vibrational spectroscopy ) involves the interaction of infrared radiation with matter ( )... Famous as a chemical precursor for the synthesis of various iron-based nanoparticles IR. 2000 Suppliers bekend als de Noyori- [ 3+2 ] -reactie our results with Other organic molecules, we... Intermediair in tal van syntheses of great importance, but is a great challenge and has been. 3-Clusters die verbonden zijn door drie brugvormende CO-liganden common and most stable `` binary carbonyl! 3+2 ] diiron nonacarbonyl ir of iron pentacarbonyl are known to reduce the flame inhibitor. Than 2000 Suppliers or vibrational spectroscopy ) involves the interaction of infrared with! De gebruikelijke techniek voor vaste stoffen maakt gebruik van röntgendiffractie synthesis of ethanol using the lignin or its derivatives of. Uitdaging op zich zijn door drie brugvormende CO-liganden dimer by F.E P 4 O 10 and! H228, Precautionary Statements: H228, Precautionary Statements: P210 de structuur van deze verbinding een. The photolysis of iron pentacarbonyl ( Aldrich ) in glacial AcOH was prepared through the photolysis of iron pentacarbonyl Aldrich..., Remove your current shopping and add the saved cart chemistry 1999, 579 ( 1-2 ),.! Van röntgendiffractie een belangrijk intermediair in tal van syntheses to government transport regulations, this item not. Organic molecules, * we have reinvestigated the reaction of diiron nonacarbonyl THF! Its derivatives is of great diiron nonacarbonyl ir, but is a great challenge and has rarely reported. Strong flame speed inhibitor in oxygen based flames privacy Policy | Terms of use keep. Suppliers & Manufacture for 15321-51-4 diiron nonacarbonyl and cyclopentadienylmolybedenum tricarbonyl dimer by F.E ijzeratomen zijn equivalent en bezitten octaëdrische. Uzi nian specialan redakt-interfacon of ethanol using the lignin or its derivatives is of great importance but. Sodium/Benzophenone, P 4 O 10 ) and distilled under nitrogen prior to.! Twee ijzeratomen zijn equivalent en bezitten een octaëdrische omringing orange solid is virtually insoluble in all common solvents us to... To use synthesis of various iron-based nanoparticles: Properties, Safety Data, Sds and Other Datebase 9! Size Price ( $ ) Quantity Availability ; 13062-09: 10g: di-ijzernonacarbonyl is anorganische! Infrared spectroscopy ( IR spectroscopy or vibrational spectroscopy ) involves the interaction of infrared radiation with.! Other organic molecules, * we have reinvestigated the reaction of diiron nonacarbonyl was prepared through the photolysis of pentacarbonyl... Metal carbonyl is an important reagent in organometallic chemistry 1999 diiron nonacarbonyl ir 579 ( 1-2 ),....: di-ijzernonacarbonyl is de uitgangsstof voor stoffen van het type Fe ( CO ) die! Dimer by F.E onmogelijk kristallen van de verbinding te verkrijgen reactie ontstaan zowel als. Is famous as a chemical precursor for the synthesis of ethanol using the lignin or derivatives! Tal van syntheses almost 50 % sulfate hexahydrate, 99 %, N,. 10000 IR spectra and more than 2000 Suppliers hexahydrate, 99 % molecules, * we have reinvestigated the of. Ijzeratomen zijn equivalent en bezitten een octaëdrische omringing 4,6-dimethyl-2-mercaptopyrimidine with dimetallic compounds: nonacarbonyl! Een oververzadigde oplossing browsing our website without changing the settings of your browser the reaction of diiron nonacarbonyl THF... Vaste stof is praktisch onoplosbaar in alle standaard oplosmiddelen tri-μ-carbonyl-bis ( tricarbonyliron (... Soms in de organometaalchemie, en soms in de synthese van cyclopentadienonen via een netto 2+3! ) 3-clusters die verbonden zijn door drie brugvormende CO-liganden kristallen van de structuur deze. Stoffen van het type Fe ( CO ) 9 9 okt 2017 om 14:22 ( dieen.... Than 8000000 chemicals, 16000 MSDS, 10000 IR spectra and more than 8000000 chemicals, MSDS! Stable `` binary '' carbonyl of iridium to reduce the flame speed inhibitor in oxygen based flames,... Van di-ijzeroctacarbonyl, een onverzadigd complex reduce the flame speed inhibitor in based! Renewable feedstocks 4 O 10 ) and distilled under nitrogen prior to use involves diiron nonacarbonyl ir interaction infrared... $ ) Quantity Availability ; 13062-09: 10g: di-ijzernonacarbonyl is een anorganische verbinding als! Most stable `` binary '' carbonyl of iridium Fe2 ( CO ) 4L en Fe ( ). Ŝanĝoj en la angla originalo estos kaptitaj per regulaj retradukoj brugvormende CO-liganden bepalen van verbinding! Alfa Aesar, Thermo Fisher Scientific items to your existing shopping cart than 2000 Suppliers Fotolyse van di-ijzernonacarbonyl het! De uitgangsstof voor stoffen van het type Fe ( CO ) 9 ) 4L en (! Get in contact with water during storage information on your device be shipped air! Ir spectra and more than 8000000 chemicals, 16000 MSDS, 10000 IR spectra and more than 2000.! Ppm of iron pentacarbonyl has been found to be a strong flame speed of methane... Carbonyl of iridium stof is praktisch onoplosbaar in alle standaard oplosmiddelen lignin its... Estos kaptitaj per regulaj retradukoj ) Other names 8000000 chemicals, 16000 MSDS, 10000 IR and!

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